UDDB Equipamento de Destilação Descontínua

11.1.4.- DESTILAÇÃO E CRAQUEAMENTO
BATCH DISTILLATION UNIT - UDDB

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EDIBON's distillation unit, in its different versions, is one of the most powerful laboratory tools for the study of the variables that affect the distillation process.

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Descrição Geral

Distillation is used to separate liquid mixtures made up of individual liquids that are soluble in one another.

EDIBON's distillation unit, in its different versions, is one of the most powerful laboratory tools for the study of the variables that affect the distillation process.

The student can investigate the principles that rule the mass and energy transference, as well as determine the optima operation point to carry out a big quantity of separations.

It is basically composed by a boiler on which two types of interchangeable columns can be adapted (plate columns and Raschig Rings column), a reflux system and a tank for the distillation.

The steam that goes to the head of the column is sent to a total condenser. The cooling water flow that crosses the condenser is regulated and indicated in a flow meter.

The pressure loss in the column can be measured with a manometer.

The temperatures of the system are measured by temperature sensors placed in strategic positions.

EXERCÍCIOS E PRÁTICAS GUIADAS

EXERCÍCIOS PRÁTICOS GUIADOS INCLUÍDOS NO MANUAL

  1. Preparation of solutions.
  2. Analytic valuation techniques.
  3. Filling of the column.
  4. Batch operation.
  5. Obtaining the McCabe-Thiele diagram. Without reflux.
  6. Obtaining the number of plates. Without reflux.
  7. Efficiency calculations. Without reflux.
  8. Variation of the composition of the distilled product: constant reflux ratio.
  9. Constant composition of the distilled product: variation of reflux ratio.
  10. Constant composition of the distilled product: constant reflux ratio.
  11. Mass and energy balances across the system.
  12. Plates fluid dynamics studies, including load loss and column flooding.
  13. Calculation of the theoretical number of floors in the plates columns, and the equivalent height of the theoretical floor (HEPT) in the Raschig rings columns.
  14. Pursuit of the temperatures in all plates in the column (Plates columns).
  15. Study of the rectification efficiency.
  16. Demonstration of azeotropic distillation.
  17. Studies of heating interchange in glass refrigerators

EQUIPAMENTOS SIMILARES DISPONÍVEIS

CONTINUOUS DISTILLATION UNIT - UDCB
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11.1.4.- DESTILAÇÃO E CRAQUEAMENTO
UDCB
Equipamento de Destilação Contínua
The Continuous Distillation Unit, "UDCB", is formed by a boiler, on which different types of columns can be adapted (plate columns and Raschig columns). An eight plate column, a reflux system, a tank for distillation, a vacuum pump and a feeding...
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